Detecting the concentrations of bisphenol A (BPA) in air of workplaces with HPLC.
- Author:
Chun-hun WU
1
;
Dong-sheng REN
;
Yong-hua HE
;
Li-xing ZHENG
;
Zhi-jun ZHOU
Author Information
- Publication Type:Journal Article
- MeSH: Air Pollutants, Occupational; analysis; Benzhydryl Compounds; Chromatography, High Pressure Liquid; methods; Environmental Monitoring; methods; standards; Phenols; analysis; Workplace
- From: Chinese Journal of Industrial Hygiene and Occupational Diseases 2011;29(11):856-858
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVETo establish the method of detecting the concentrations of bisphenol A (BPA)in air of workplaces with high performance liquid chromatographic (HPLC).
METHODSAccording to standards of methods for determining the chemical substances in workplace air, BPA in the air was collected by glass fiber filter, then dissolved by acetonitrile and determined by high performance liquid chromatography with FLD.
RESULTSThere was a linear relationship within the range of 0.01-10.0 pg /ml, and the detection limit was 0.005 pg/ml. The lowest detected concentration was 3.3x10-5 mg/m3. The relative standard deviation was 2.5-5.5%. The dissolution efficiencies were 95.0%-101.9% and the sampling efficiencies were 99.6%. The samples in glass fiber filter membrane could be stored for 7 days at room temperature.
CONCLUSIONThe present method could meet with the requirements of Guide for establishing occupational health standards-Part 4 Determination methods of air chemicals in workplace and be feasible for determination of BPA in workplace air.