Studies on lignan constituents of Clematis parviloba.
- Author:
Li-hua YAN
1
;
Li-zhen XU
;
Jia LIN
;
Zhong-mei ZOU
;
Bao-hua ZHAO
;
Shi-lin YANG
Author Information
- Publication Type:Journal Article
- MeSH: Chromatography, Gel; Chromatography, High Pressure Liquid; Clematis; chemistry; Drugs, Chinese Herbal; chemistry; isolation & purification; Furans; chemistry; isolation & purification; Glucosides; chemistry; isolation & purification; Lignans; chemistry; isolation & purification; Magnetic Resonance Spectroscopy; Plant Stems; chemistry; Spectrometry, Mass, Electrospray Ionization
- From: China Journal of Chinese Materia Medica 2008;33(15):1839-1843
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVETo study the chemical constituents of the stems of Clematis parviloba.
METHODThe compounds were isolated and purified by repeated column chromatography with silica gel, Sephadex LH-20 and HPLC. Their structures were identified by spectroscopic data together with physical and chemical property.
RESULTTen compounds have been isolated from the stems of C. parviloba, and identified as: (+) pinoresionol (1), (+) pinoresionol-4'-O-p-D-glucopyranoside (2), ( +) pinoresionol4, 4'-O-bis-beta-D-glucopyranoside (3), (-) syringaresinol (4), (+) syringaresinol-4'-O-beta-D-glucopyranoside (5), (-)episyringaresinol (6), (+) medioresinol-4'-O-beta-D-glucopyranoside (7), (+) lariciresinol-4-O-beta-D-glucopyranoside (8), (+) lariciresinol-4'-O-beta-D-glucopyranoside (9), (+) lariciresinol-4, 4'-O-bis-beta-D-glucopyranoside (10), respectively.
CONCLUSIONCompounds 6, 7 were isolated from this genus for the first time, and the other ones were isolated from this plant for the first time.
