Purification of total flavones from Bushen Recipe with macroporous resin
- VernacularTitle:大孔吸附树脂纯化补肾方中总黄酮的工艺研究
- Author:
Wanzhong SHI
;
Jin LIU
;
Haiyang L
;
Desheng XU
;
Li LIU
- Publication Type:Journal Article
- Keywords:
Bushen Recipe;
macroporous resin;
total flavones;
icariin;
tetrahydroxystilbene;
naringin
- From:
Chinese Traditional Patent Medicine
1992;0(07):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM: To study the absorption performance and purification process of total flavones from Bushen Recipe(Radix polygoni multiflori;Herba epimedii;Rhizoma drynariae;etc) with macroporous resin. METHODS: The contents of total flavones,icariin,tetrahydroxystilbene and naringin were worked as indexes,the adsorptive capacity of D101,DA201 and DM301 resins were investigated,and the static adsorption curve,dynamic leakage curve and elution curve were used for the selection of macroporous resin. RESULTS: The elution parameters of selected DM301 consisted of the 0.25 BV/h feed rate solution ratio of 4 BV water to elute resin and 4 BV 70% alcohol to be collected as elution solvent,and the elution rate of 2.4 BV/h was established. CONCLUSION: Macroporous resin method is a better candidate method for purifying flavones in Bushen Recipe.
